HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 18645595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 4,4-Dimethylcholest-7-en-3-ol | HCID 5460076 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18645595 | HCID 18645595 | — |
Reaction Steps
4,4-Dimethyl-5α-cholest-7-en-3β-ol [prepared according to J. Biol. Chem., 233:1343 (1958)]was converted to the title compound with benzoyl chloride in pyridine at ambient temperature for 18 hours. 3β-benzoyloxy-4,4-dimethyl-5α-cholest-7-ene had an mp of 160°-161° C. (from CH2Cl2/MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023250 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-da4ee7ccae7241ff8f9d33bb620d7a4e |
| Source note | uspto-grants-1991_06 |