HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenoxybenzoic acid hydrazide → HCID 53690311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenoxybenzoic acid hydrazide | HCID 142650 | — |
| Reactant | 3-methyl-1-(pyridin-4-yl)butan-1-one | HCID 14742852 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Product | HCID 53690311 | HCID 53690311 | — |
Reaction Steps
Following the general method of procedure 4 and making noncritical variations, except 12 drops of glacial acetic acid is added as a catalyst, 9.00 gm (0.055 mole) of isobutyl 4-pyridyl ketone and 12.59 gm (0.055 mole) of 2-phenoxybenzhydrazide yield 13.89 gm (67%) of the title compound having a melting point of 137.6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023334 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-5a55bcaeb59d42a4862eff2c5f892475 |
| Source note | uspto-grants-1991_06 |