HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 5-(4-Chlorophenyl)furan-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 5-(4-chlorophenyl)furan-2-carbonyl Chloride | HCID 2771970 | — |
| Product | 5-(4-Chlorophenyl)furan-2-carboxamide | HCID 4780001 | — |
Reaction Steps
To 1000 ml. of cold, stirring NH4OH, 63 g. (0.26 mole) of 5-(p-chlorophenyl)-2-furoyl chloride is added portionwise. The resulting mixture is stirred at ice bath temperature for 15 minutes and then is stored at room temperature for 18 hours. The solid is filtered, is washed with water and is dried at 60° to yield 56 g. (97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023272 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-2245ed9770494de7b665cb3ba76866c2 |
| Source note | uspto-grants-1991_06 |