2-(4-Chlorophenoxy)ethanol → 2-(4-Chlorophenoxy)ethanol sulfamate

HRID 1493979Notes

Reaction equation

HRID 1493979 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][OH:14])=[CH:9][CH:8]=1>>[Cl:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][O:14][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:9][CH:8]=1

Participants

3

Reactant 2

HCID 159072-(4-Chlorophenoxy)ethanolHCID 24499Chlorosulfamic acid

Product 1

HCID 191086672-(4-Chlorophenoxy)ethanol sulfamateYield 48%

Procedure

The title compound was prepared by procedures of Example 4 from sulfamoyl chloride and 2-(4-chlorophenoxy)ethanol in 48% yield. A white solid, mp 117°-119° C., was obtained.

Workup

  1. customA white solid, mp 117°-119° C., was obtained

Sources & evidence

ORD record
ord-d285a744abd34ee9a28c188085c0bf23
Source dataset
uspto-grants-1991_06
Patent number
US05025031

Reaction notes

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