Chlorosulfamic acid → HCID 19108682, compound

HRID 1493983Notes

Reaction equation

HRID 1493983 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][O:7][C:8]1[CH:17]=[CH:16][C:11]([O:12][CH2:13][CH2:14][OH:15])=[CH:10][CH:9]=1>>[CH3:6][O:7][C:8]1[CH:17]=[CH:16][C:11]([O:12][CH2:13][CH2:14][O:15][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 2200792-(4-Methoxyphenoxy)ethanol

Product 1

HCID 19108682HCID 19108682, compoundYield 54%

Procedure

The title compound was prepared by procedures of Example 16 from sulfamoyl chloride and 2-(4-methoxyphenoxy)ethanol in 54% yield as an off-white solid, mp 84°-87° C.

Sources & evidence

ORD record
ord-7f1c4065b4564284bcabc5950fc5b943
Source dataset
uspto-grants-1991_06
Patent number
US05025031

Reaction notes

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