Phenol → Phenylsulfamate

HRID 1493985Notes

Reaction equation

HRID 1493985 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[C:6]1([OH:12])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([O:12][S:1](=[O:4])(=[O:3])[NH2:2])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 996PhenolHCID 24499Chlorosulfamic acid

Product 1

HCID 11030308PhenylsulfamateYield 30%

Procedure

The compound was prepared by procedures of Example 16 from sulfamoyl chloride and phenol in 30% yield as white solid, mp 81°-85° C.

Sources & evidence

ORD record
ord-3896d3af38d84bae911e2c9372a0ff93
Source dataset
uspto-grants-1991_06
Patent number
US05025031

Reaction notes

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