HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorophenol → HCID 19108716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorophenol | HCID 7933 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Product | HCID 19108716 | HCID 19108716 | 7.6% |
Reaction Steps
By the procedure of Example 34,96 g (0.75 mole) of 3-chlorophenol and 67.5 ml (0.75 mole) of chlorosulfonyl isocyanate gave 122.9 g of solid product. A 25 g portion was recrystallized from 100 ml of toluene to give 11.8 g of white solid, mp 82°-83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-845bd7c845d2482ebe33c56bebca2fa7 |
| Source note | uspto-grants-1991_06 |