HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenol → HCID 10059221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenol | HCID 11137 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10059221 | HCID 10059221 | — |
Reaction Steps
This compound was prepared according to the procedure used in Example 56. A mixture of 13.9 g (0.1 mole) of 3-nitrophenol and 14.8 g (0.105 mole) of chlorosulfonyl isocyanate in 100 ml of toluene gave 16.9 g (78%) of tan flakes, mp 118°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-cca3ee606dfd481cb63f6c336df8d180 |
| Source note | uspto-grants-1991_06 |