HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylphenol → Phenylacetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylphenol | HCID 11381 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Phenylacetonitrile | HCID 8794 | — |
| Product | HCID 54439888 | HCID 54439888 | — |
Reaction Steps
Using the procedure described in Example 56, the title compound was prepared from 17.0 g (0.010 mole) of 3-phenylphenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 100 ml of toluene to obtain 19.0 g (77%) of white flakes, mp 197°-199° C. (benzene-acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-94097e43ac17488fafb3cc638911b19f |
| Source note | uspto-grants-1991_06 |