Chlorosulfonyl isocyanate → HCID 46883000, compound

Participants

Reaction Steps

Using the procedure of Example 56, the title compound was prepared using a mixture of 9.9 g (0.076 mole) of 3,5-difluorophenol and 7.0 ml (0.08 mole) of chlorosulfonyl isocyanate in 50 ml of toluene. The solid product was recrystallized from benzene to yield 11.7 g (74%) of white solid, mp 85°-88° C.

Provenance & Evidence