HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenol → 4-Fluorophenyl sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 4-Fluorophenyl sulfamate | HCID 44459223 | — |
Reaction Steps
Using the procedure of Example 56, a mixture of 11.2 g (0.1 mole) of 4-flurophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 50 ml of toluene gave, after recrystallization from benzene, 15.0 g (79%) of the title compound as a white solid, mp 82.5°-85.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025031 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-57104256eff64a349cdeec91572a6b3c |
| Source note | uspto-grants-1991_06 |