HRID1494225

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCCc1cc(C(=O)OCC)cc(CCC)c1OCCCCCCc1cccc(OC)c1OC

HCID14986323

未命名化合物

PRODUCTS

生成物

结构：CCCc1cc(C(=O)O)cc(CCC)c1OCCCCCCc1cccc(OC)c1OC

HCID14986324

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

溶剂HCID14798

Sodium Hydroxide

HNaO

PROCEDURE

实验过程

A solution of 1.8 g of 4-[6-(2,3-dimethoxyphenyl)hexyloxy]-3,5-dipropylbenzoic acid ethyl ester in 100 mL of methanol and 20 mL of 1N sodium hydroxide was stirred at reflux for 3 hours. Workup as in Example 24 gave 4-[6-(2,3-dimethoxyphenyl)hexyloxy]-3,5-dipropylbenzoic acid, mp 61°-65°.

WORKUP

后处理

temperatureat reflux for 3 hours