HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[6-[2,3-Bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid methyl ester → 3-[6-[2,3-Bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[6-[2,3-Bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid methyl ester | HCID 14986346 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 3-[6-[2,3-Bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid | HCID 14986347 | 70% |
Reaction Steps
A solution of 0.5 g of 3-[6-[2,3-bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid methyl ester in 15 mL of methanol and 5 mL of 1N sodium hydroxide was stirred at reflux for 2 hours. Workup as in Example 24 and crystallization from methanol gave 0.34 g (70% yield), mp 72°-74°of 3-[6-[2,3-bis(phenylmethoxy)phenyl]hexyloxy]benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05025036 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-aa934d16f6a6425a9f43c65cc1bdeab9 |
| Source note | uspto-grants-1991_06 |