Acetic Acid → HCID 67922900, compound

Participants

Reaction Steps

5.2 g (0.02 mol) of 3-nitro-4-(β-bromoethyl)-aminophenol are heated for 1 hour, at 60° C., in 20 ml of diethanolamine. The reaction medium is poured into 100 g of iced water and the solution is then neutralised with acetic acid. After one night at 0° C., the expected product, which has precipitated, is filtered off. After washing with a small amount of iced water and drying in vacuo, the product is recrystallised from ethyl acetate. It melts at 115° C.

Provenance & Evidence