HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzenamine, N-methyl-2-nitro-4-(trifluoromethyl)- → N1-Methyl-4-(trifluoromethyl)benzene-1,2-diamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzenamine, N-methyl-2-nitro-4-(trifluoromethyl)- | HCID 88405 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N1-Methyl-4-(trifluoromethyl)benzene-1,2-diamine | HCID 715666 | — |
Reaktionsschritte
A solution of 1.1 g (5.0 mmol) 4-methylamino-3-nitrobenzotrifluoride in 200 ml ethanol was hydrogenated at atm. pressure by using 5% Pd-C (0.15 g) as a catalyst. The reaction mixture was filtered and evaporated in vacuo to give 3-amino-4-methylaminobenzotrifluoride as crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05026704 |
| Quelldatensatz | uspto-grants-1991_06 |
| ORD ID | ord-a396ad32849a490e9186704cb2ea1347 |
| Quellennotiz | uspto-grants-1991_06 |