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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1494334Erstellt: 25. Oktober 2026

Benzenamine, N-methyl-2-nitro-4-(trifluoromethyl)- → N1-Methyl-4-(trifluoromethyl)benzene-1,2-diamine

https://huagongshe.com/reaction/1494334

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzenamine, N-methyl-2-nitro-4-(trifluoromethyl)-HCID 88405—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
ProduktN1-Methyl-4-(trifluoromethyl)benzene-1,2-diamineHCID 715666—

Reaktionsschritte

A solution of 1.1 g (5.0 mmol) 4-methylamino-3-nitrobenzotrifluoride in 200 ml ethanol was hydrogenated at atm. pressure by using 5% Pd-C (0.15 g) as a catalyst. The reaction mixture was filtered and evaporated in vacuo to give 3-amino-4-methylaminobenzotrifluoride as crystals.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05026704
Quelldatensatzuspto-grants-1991_06
ORD IDord-a396ad32849a490e9186704cb2ea1347
Quellennotizuspto-grants-1991_06