HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl cyclopropyl ketone → HCID 13764025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl cyclopropyl ketone | HCID 81148 | — |
| Reactant | HCID 178437635 | HCID 178437635 | — |
| Product | HCID 13764025 | HCID 13764025 | — |
Reaction Steps
Combine 25 g (0.14 mol) of 4-chlorophenyl cyclopropyl ketone with 50 g (0.45 mol) of 2-ethyl-4-methylimidazole, and heat to 175° C. under argon for 40 hr. Isolate the title compound by column chromatography on 500 g of silica gel using 1% methanol/methylene chloride as solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026712 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-ffacdda0f7ba48ce98feda567b1e9682 |
| Source note | uspto-grants-1991_06 |