HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 86744867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 8-Chloro-1,2,3,4-tetrahydronaphthalen-2-one | HCID 4623269 | — |
| Product | HCID 86744867 | HCID 86744867 | — |
Reaction Steps
Using the method of Example 3, 0.5 g (2.78 mmol) of 8-chloro-2-tetralone was treated with N-methylpiperazine, and the resulting product was reduced with sodium borohydride and the product treated with maleic acid to obtain 0.48 g of the title compound as colorless crystals, m.p. 199°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026707 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-11eaef04edfc46238c00182a1db2722c |
| Source note | uspto-grants-1991_06 |