HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cfc 113 → HCID 14912590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cfc 113 | HCID 6428 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 14912585 | HCID 14912585 | — |
| Product | HCID 14912590 | HCID 14912590 | 82% |
Reaction Steps
A solution of 118 g (0.52 mol) of 3 in 200 mL of CFCl2CF2Cl was stirred under a -80° condenser and irradiated with a sunlamp while chlorine was passed in until reaction ceased. Distillation gave 127.4 g (82%) of 2,2,3,3-tetrachloro-5,5,6,6-tetrafluoro-1,4-dioxane (4), bp 65° C. (40 mm)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026801 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-adb683ee098e429faae37d7d35b709a1 |
| Source note | uspto-grants-1991_06 |