N-Phenyl-m-anisidine → 4-Methoxy-10H-phenothiazine

HRID 1494505Notes

Reaction equation

HRID 1494505 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([NH:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=1.COC1C=CC2[S:28]C3C(=CC=CC=3)NC=2C=1>>[CH3:1][O:2][C:3]1[C:8]2[S:28][C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[NH:9][C:7]=2[CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 7544N-Phenyl-m-anisidineHCID 74490Methyl phenothiazin-2-yl ether

Product 1

HCID 198283464-Methoxy-10H-phenothiazine

Procedure

The conversion rate of the 3-methoxydiphenylamine is 91%, and the chemical yield of 2-methoxyphenothiazine is 91%.

Sources & evidence

ORD record
ord-9d28eb95d5ea47f6934f3116e70fe92f
Source dataset
uspto-grants-1991_06
Patent number
US05026846

Reaction notes

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