HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → (3-Formyl-4-hydroxyphenyl)methyl 2-methylprop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | 5-(Chloromethyl)-2-hydroxybenzaldehyde | HCID 335291 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | (3-Formyl-4-hydroxyphenyl)methyl 2-methylprop-2-enoate | HCID 20095941 | — |
Reaction Steps
5-Chloromethylsalicylaldehyde (34 g) (prepared by the method of Angyal et al., J. Chem. Soc. 2141, (1950)) was added to a stirred mixture of acetone (250 ml), sodium hydrogen carbonate (33.6 g), and methacrylic acid (34.4 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05026860 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-ba985160dd0047a7aca4cd490c715933 |
| Source note | uspto-grants-1991_06 |