Isopropanol → HCID 86744877, compound

Participants

Reaction Conditions

Reaction Steps

2,5-Dimercapto-1,3,4-thiadiazole(79.9 grams, 0.53 moles) was charged into a reaction flask followed by isopropanol solvent, 200 ml. The epoxide, dodecyl glycidyl ether (272.4 grams, 1.06 moles) was added slowly to the reactor with stirring. The reaction mixture was heated at about 80° C. for 0.5 hours. At this time the solvent was stripped by using a rotary evaporator at approximately 20 mm Hg and 100° C. The product was a low melting solid characterized by the infrared absorption bands at 3400, 2900, 1460, 1380, 1120, and 1050 cm-1.

Provenance & Evidence