Isopropanol → HCID 15144524, compound

Participants

Reaction Steps

In a reaction flask, isopropanol (100 ml),dodecylmercaptan (30.66 grams, 0.151 moles),and sodium hydroxide pellets(6.1 grams, 0.153 moles) were mixed with stirring. In another flask 2,5-dimercapto-1,3,4-thiadiazole (11.3 grams, 0.076 moles) and epichlorohydrin(14 grams, 0.151 moles) were reacted in isopropanol(100 ml) by heating to reflux temperature. The reacted mixture was added to the reaction flask and refluxed for 0.5 hours. The solvent was stripped off to produce a yellow oil product characterized by the infrared absorption bands at 3400, 2900, 1680, 1460, 1380, 1040, and 720 cm-1.

Provenance & Evidence