HRID1494600

反应详情

EQUATION

反应方程式

HRID 1494600 的结构方程式

PROCEDURE

实验过程

A mixture 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid (5.09 g) and thionyl chloride (25 ml) was refluxed for 10 hours. Excess thionyl chloride was distilled off under reduced pressure. The crude product was used as such for the following reaction.

WORKUP

后处理

  1. distillationExcess thionyl chloride was distilled off under reduced pressure
  2. customsuch for the following reaction