Thionyl Chloride → HCID 53915754, compound

HRID 1494600Notes

Reaction equation

HRID 1494600 reaction equation
[CH:1]([C:3]1([C:12]([OH:14])=O)[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].S(Cl)([Cl:17])=O>>[CH:1]([C:3]1([C:12]([Cl:17])=[O:14])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 19828700HCID 19828700, compound

Product 1

HCID 53915754HCID 53915754, compound

Procedure

A mixture 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid (5.09 g) and thionyl chloride (25 ml) was refluxed for 10 hours. Excess thionyl chloride was distilled off under reduced pressure. The crude product was used as such for the following reaction.

Workup

  1. distillationExcess thionyl chloride was distilled off under reduced pressure
  2. customsuch for the following reaction

Sources & evidence

ORD record
ord-89f5ee2aa9fd40c395f9ef973cc3e60a
Source dataset
uspto-grants-1991_06
Patent number
US05026868

Reaction notes

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