Nitrobenzene → Nonane

HRID 1494696Notes

Reaction equation

[N+](C1C=CC=CC=1)([O-])=O.[C:10]([CH2:13][C:14]1C2[C:18](=[CH:19]C=CC=2)[CH:17]=[CH:16][CH:15]=1)(=O)[CH3:11]>>[CH3:11][CH2:10][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

Reactant 2

HCID 7416Nitrobenzene

HCID 3496831-naphthylacetone

Product 1

HCID 8141Nonane

Procedure

A crude isomer mixture weighing 33.71 grams and containing 59.4 weight percent 2,6-AMN, 12.8 weight percent nitrobenzene and 27.8 weight percent of other materials which were believed to be mainly other isomers of acetylmethylnaphthalene was used for the present evaluation.

Workup

additioncontaining 59.4 weight percent 2,6-AMN

Sources & evidence

ORD record: ord-efb7ec0b91a6488cb8ced6a3e8c4295b
Source dataset: uspto-grants-1991_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05026917

Reaction notes

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