HRID1496813

反应详情

EQUATION

反应方程式

HRID 1496813 的结构方程式

PROCEDURE

实验过程

The 9-dodecenoic acid methyl ester is then hydrolyzed under basic conditions (reflux with an excess of dilute aqueous NaOH), followed by removal of methanol. The resulting aqueous solution is then treated with an excess of dilute HCl, and the solution is distilled to provide 9-dodecenoic acid. Estolides are then prepared according to the methods set forth in Examples 1 and 2, wherein the oleic acid is replaced with 9-dodecenoic acid.

WORKUP

后处理

  1. customfollowed by removal of methanol
  2. additionThe resulting aqueous solution is then treated with an excess of dilute HCl
  3. distillationthe solution is distilled