HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118105751, compound → HCID 63672100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118105751 | HCID 118105751 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 63672100 | HCID 63672100 | — |
Reaction Steps
The compound prepared in Step 2 was dissolved in ethanol, added with 10% Pd/C and stirred under hydrogen atmosphere for 2 hours. Upon completion of the reaction, the Pd/C in the reaction mixture was removed using celite and the solvent was removed under reduced pressure. The thus obtained compound was used in the subsequent reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199944B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-cc438745aeca4ecd9e2fa9c0048a10c4 |
| Source note | uspto-grants-2015_12 |