N-Methylisopropylamine → HCID 71556556, compound

HRID 1497118Notes

Reaction equation

HRID 1497118 reaction equation
C[O:2][C:3]([C:5]1[C:6](Cl)=[N:7][C:8]2[C:13]([C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:12][C:11]([Cl:21])=[CH:10][C:9]=2[Cl:22])=[O:4].[CH:24]([NH:27][CH3:28])([CH3:26])[CH3:25]>>[Cl:21][C:11]1[CH:12]=[C:13]2[C:8](=[C:9]([Cl:22])[CH:10]=1)[N:7]=[C:6]([N:27]([CH:24]([CH3:26])[CH3:25])[CH3:28])[C:5]([C:3]([OH:2])=[O:4])=[C:14]2[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 78485N-MethylisopropylamineHCID 86682943HCID 86682943, compound

Product 1

HCID 71556556HCID 71556556, compound

Procedure

The title compound was prepared in analogy to example 21 step D from 2,6,8-trichloro-4-phenyl-quinoline-3-carboxylic acid methyl ester (prepared as described in example 21 step C) and isopropyl-methyl-amine. Light brown foam. MS (ESI): 389.2 (M+H)+.

Sources & evidence

ORD record
ord-ecfa711b096e48fc91bd0aaaf7775465
Source dataset
uspto-grants-2015_12
Patent number
US09199938B2

Reaction notes

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