N-Methylethylamine → HCID 71556619, compound

HRID 1497125Notes

Reaction equation

C[O:2][C:3]([C:5]1[C:6](Cl)=[N:7][C:8]2[C:13]([C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:12][C:11]([Cl:21])=[CH:10][C:9]=2[Cl:22])=[O:4].[CH2:24]([NH:26][CH3:27])[CH3:25]>>[Cl:21][C:11]1[CH:12]=[C:13]2[C:8](=[C:9]([Cl:22])[CH:10]=1)[N:7]=[C:6]([N:26]([CH2:24][CH3:25])[CH3:27])[C:5]([C:3]([OH:2])=[O:4])=[C:14]2[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

Participants

Reactant 2

HCID 12219N-Methylethylamine

HCID 86682943HCID 86682943, compound

Product 1

HCID 71556619HCID 71556619, compound

Procedure

The title compound was prepared in analogy to example 21 step D from 2,6,8-trichloro-4-phenyl-quinoline-3-carboxylic acid methyl ester (prepared as described in example 21 step C) and ethyl-methyl-amine. Brown foam. MS (ESI): 375.1 (M+H)+.

Sources & evidence

ORD record: ord-772ec017d41243c9952521251438a0f5
Source dataset: uspto-grants-2015_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09199938B2

Reaction notes

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