Benzenamine, 4-chloro-2-(trifluoromethyl)- → HCID 66865667, compound

HRID 1497187Notes

Reaction equation

HRID 1497187 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH2:8])=[C:4]([C:9]([F:12])([F:11])[F:10])[CH:3]=1.[I:13]N1C(=O)CCC1=O>>[Cl:1][C:2]1[CH:3]=[C:4]([C:9]([F:10])([F:11])[F:12])[C:5]([NH2:8])=[C:6]([I:13])[CH:7]=1

Participants

3

Reactant 2

HCID 67961Benzenamine, 4-chloro-2-(trifluoromethyl)-HCID 120273N-Iodosuccinimide

Product 1

HCID 66865667HCID 66865667, compound

Procedure

The title compound was prepared in analogy to example 76 step A from 4-chloro-2-trifluoromethyl-phenylamine (1 g, 5.11 mmol) and N-iodo succinimide (1.73 g, 7.67 mmol). Off white solid. (1.64 g, 88%). GC-MS: 321 (M).

Sources & evidence

ORD record
ord-46ee168f30784561a5bc042fdbf66e42
Source dataset
uspto-grants-2015_12
Patent number
US09199938B2

Reaction notes

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