HRID1497396

反应详情

EQUATION

反应方程式

HRID 1497396 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A suspension of 4-(benzyloxy)-1-(2-ethyl-3-methyl-2H-indazol-5-yl)pyridin-2(1H)-one (1.5 g) and 10% palladium carbon (444 mg) in methanol (30 ml) was stirred under a hydrogen atmosphere at room temperature for 3 hr. The insoluble material was filtered off, and the obtained filtrate was concentrated under reduced pressure to give the title compound (1.07 g).

WORKUP

后处理

  1. filtrationThe insoluble material was filtered off
  2. concentrationthe obtained filtrate was concentrated under reduced pressure