3-Fluoro-4-methoxyphenylboronic acid → HCID 69671330, compound

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Reaction Steps

The title compound was prepared form 6-chloro-3-(4-chloro-2-methoxyphenyl)-[1,2,4]triazolo[4,3-a]pyridine and 3-fluoro-4-methoxyphenylboronic acid using a procedure similar to those described for the synthesis of Example 1d, and was isolated as white solids. 1H NMR (DMSO-d6): 8.29 (m, 1H), 7.92 (dd, J=9.6 and 0.9 Hz, 1H), 7.80 (dd, J=9.6 and 1.8 Hz, 1H), 7.71-7.62 (m, 2H), 7.56 (m, 1H), 7.54 (t, J=1.2 Hz, 1H), 7.40-7.23 (m, 2H), 3.88 (s, 3H), 3.87 (s, 3H). MS: m/z 384.2 [M+H+].

Provenance & Evidence