2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol → HCID 69671281, compound

Participants

Reaction Steps

The title compound was prepared from 6-chloro-3-(2-methoxy-4-methylphenyl)-[1,2,4]triazolo[4,3-a]pyridine and 2-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol using a procedure similar to those described for the synthesis of Example 1d, and was isolated as yellow solids. 1H NMR (DMSO-d6): 9.23 (s, 1H), 7.91-7.86 (m, 2H), 7.69 (dd, J=9.6 and 1.5 Hz, 1H), 7.49 (d, J=7.5 Hz, 1H), 7.16-6.99 (m, 5H), 3.84 (s, 3H), 3.80 (s, 3H), 2.45 (s, 3H). MS: m/z 362.2 [M+H+].

Provenance & Evidence