huagongshe.com
HRID1497602

反应详情

EQUATION

反应方程式

HRID 1497602 的结构方程式

REACTANTS

反应物

2
结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1ccc(C2OCCO2)o1
HCID10960952

Stannane, tributyl[5-(1,3-dioxolan-2-yl)-2-furanyl]-

C19H34O3Sn

结构：Cl.O=S(=O)(c1ccccc1)N(c1ccccc1)c1ncnc2cc(F)c(I)cc12
HCID68594451

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(c1ccccc1)N(c1ccccc1)c1ncnc2cc(F)c(-c3ccc(C4OCCO4)o3)cc12
HCID21951927

未命名化合物

PROCEDURE

实验过程

Prepared according to Procedure B from (4-benzenesulphonyl)phenyl-(6-iodo-7-fluoro-quinazolin-4-yl)-amine hydrochloride and 5-(1,3-dioxolan-2-yl)-2-(tributylstannyl)furan. δ1H NMR (400 MHz, DMSO-d6) 10.49 (s, 1H), 8.88 (d, 1H), 8.63 (s, 1H), 8.1 (d, 2H), 7.95 (m, 4H), 7.65 (m, 4H), 6.97 (m, 1H), 6.75 (d, 1H), 6.01 (s, 1H), 4.09 (m, 2H), 3.97 (m, 2H). ESI-MS m/z 516 (M−1).

WORKUP

后处理

  1. customPrepared