HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 117926974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | (2-(Methylthio)ethyl)amine | HCID 87697 | — |
| Reactant | 5-(4-((4-Benzenesulphonyl-phenyl)amino)-pyrido[3,4-d]pyrimidin-6-yl)-furan-2-carbaldehyde | HCID 21951916 | — |
| Product | HCID 117926974 | HCID 117926974 | — |
Reaction Steps
5-(4-((4-Benzenesulphonyl-phenyl)amino)-pyrido[3,4-d]pyrimidin-6-yl)-furan-2-carbaldehyde (250 mg) and (methylthio)ethylamine (185 mg)) in dichloromethane (5 ml) were reacted together as in Procedure D. Purification using a Bond Elut™ cartridge, gave a yellow solid (245 mg), 70 mg of which was converted to the hydrochloride salt, (yellow solid, 68 mg); m/z 532 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199973B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-bd9132d2cf13463ab2821bbc83868953 |
| Source note | uspto-grants-2015_12 |