HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1497744Generated: October 30, 2026
Trichloroacetyl chloride → HCID 117600055, compound
https://huagongshe.com/reaction/1497744
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trichloroacetyl chloride | HCID 6420 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Amino-6-methoxybenzaldehyde | HCID 22326715 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 117600055 | HCID 117600055 | — |
Reaction Steps
A mixture of 2-Amino-6-methoxy-benzaldehyde (6.00 g, 0.04 mol) and triethylamine (4.4 g, 0.044 mol) is dissolved in THF (20 mL) and cooled to 0° C., then CCl3COCl (7.95 g, 0.044 mol) is added and stirred at 25° C. for 24 h. The mixture is extracted from water with ethylacetate to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09199988B2 |
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| Source dataset | uspto-grants-2015_12 |
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| ORD ID | ord-8d97ceb9e4554af7b8899698d5190ffc |
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| Source note | uspto-grants-2015_12 |
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