HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 73052712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | 4-{5-[2-Amino-7-methyl-8-(3-trifluoromethyl-phenyl)-[1,2,4]triazolo[1,5-a]pyridin-6-yl]-pyrazol-1-yl}-benzonitrile | HCID 73050976 | — |
| Reactant | HCID 86708108 | HCID 86708108 | — |
| Product | HCID 73052712 | HCID 73052712 | — |
Reaction Steps
The title compound was prepared from 4-{5-[2-amino-7-methyl-8-(3-trifluoromethyl-phenyl)-[1,2,4]triazolo[1,5-a]pyridin-6-yl]-pyrazol-1-yl}-benzonitrile (Ex. 1, 100 mg, 0.218 mmol) and ethyl isocyanate (90 μL, 1.089 mmol) using a similar method to that employed in Intermediate 21 (27 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09199984B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-be71cdf8e3d04348bcdde3ccdb6a8821 |
| Source note | uspto-grants-2015_12 |