HRID1498918
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
N-aminophthalimide (1.62 g) and 4-methoxy-3-methylbenzaldehyde (1.50 g) were added to ethanol (20 ml), the mixture was stirred under heat reflux overnight. The mixture was allowed to cool to a room temperature, and then the precipitate was separated by filtration, washed with ethanol, and dried under a reduced pressure to give the title compound (2.50 g, 84%).
WORKUP
后处理
- temperatureunder heat
- temperaturereflux overnight
- customthe precipitate was separated by filtration
- washwashed with ethanol
- customdried under a reduced pressure