HRID1498918

反应详情

EQUATION

反应方程式

HRID 1498918 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

N-aminophthalimide (1.62 g) and 4-methoxy-3-methylbenzaldehyde (1.50 g) were added to ethanol (20 ml), the mixture was stirred under heat reflux overnight. The mixture was allowed to cool to a room temperature, and then the precipitate was separated by filtration, washed with ethanol, and dried under a reduced pressure to give the title compound (2.50 g, 84%).

WORKUP

后处理

  1. temperatureunder heat
  2. temperaturereflux overnight
  3. customthe precipitate was separated by filtration
  4. washwashed with ethanol
  5. customdried under a reduced pressure