HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovanillin → HCID 86679348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | HCID 3298879 | HCID 3298879 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86679348 | HCID 86679348 | 68.1% |
Reaction Steps
In ethanol (3 ml), 5-(2-chlorophenyl)-2H-pyrazole-3-carboxylic acid hydrazide (30 mg) prepared in the Step 22-1-3 and 3-hydroxy-4-methoxybenzaldehyde (25 mg) was heated under reflux for 24 hours. After the mixture was allowed to cool, the precipitated crystal was separated by filtration and dried to give the title compound (32 mg, 68%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09200008B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-8713ffaae0e348229beb6936cf5c95e6 |
| Source note | uspto-grants-2015_12 |