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HRID1499129

反应详情

EQUATION

反应方程式

HRID 1499129 的结构方程式

REACTANTS

反应物

2
结构：C1COCCO1.Cl
HCID20443148

1,4-Dioxane hydrochloride

C4H9ClO2

结构：CCOC(=O)[C@@H]1CC2(CCNCC2)CN1C(=O)OCc1ccccc1
HCID117941765

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)[C@@H]1CC2(CCNCC2)CN1C(=O)OCc1ccccc1.Cl
HCID117941862

未命名化合物

PROCEDURE

实验过程

(S)-2-Benzyl 3-ethyl 2,8-diazaspiro[4.5]decane-2,3-dicarboxylate (2.4 g, 6.9 mmol) in HCl/dioxane (50 mL, 3.3 N) was stirred for 2 h at RT. The solvent was then removed in vacuo to provide (S)-2-benzyl 3-ethyl 2,8-diazaspiro[4.5]decane-2,3-dicarboxylate hydrochloride which was used directly without further purification.

WORKUP

后处理

  1. customThe solvent was then removed in vacuo