Acetic Anhydride → HCID 86729983, compound
Reaction equation
C(OC(=O)C)(=O)C.[CH3:8][C:9](=[CH:15][CH2:16][CH2:17][CH:18]([CH3:21])[CH:19]=[CH2:20])[CH2:10][CH2:11][CH:12]=[N:13]O>>[CH3:8][C:9](=[CH:15][CH2:16][CH2:17][CH:18]([CH3:21])[CH:19]=[CH2:20])[CH2:10][CH2:11][C:12]#[N:13]Participants
3
Procedure
<12> The method for producing 4,8-dimethyl-4,9-decadienenitrile according to the item <11>, wherein the dehydration step is carried out by the acetic anhydride method in which 4,8-dimethyl-4,9-decadienal oxime (an oxime intermediate) is dehydrated by heating in the presence of acetic anhydride to yield 4,8-dimethyl-4,9-decadienenitrile.
Sources & evidence
- ORD record
- ord-773b790f304e4117b743d71a7a745ee0
- Source dataset
- uspto-grants-2015_12
- Patent number
- US09200237B2
Reaction notes
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