Butanal → HCID 12026491, compound

Participants

Reaction Steps

The title compound was prepared from butyraldehyde and (E)-(2-nitrovinyl)-benzene according to the general procedure. The enantiomeric ratio was determined by HPLC with an OD-H column at 220 nm (2-propanol:hexane=5:95), 1.0 mL/min; major enantiomer tmajor=40.61 min, minor enantiomer tminor=51.74 min. The diastereomeric excess was determined by 1H NMR. [α]D20=−99.5 (c=1.1, CHCl3).

Provenance & Evidence