HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butanal → HCID 58500187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butanal | HCID 261 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 37630-26-5 | HCID 5381679 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 58500187 | HCID 58500187 | — |
Reaction Steps
The title compound was prepared from butyraldehyde and (E)-1-(2-nitrovinyl)naphthalene according to the general procedure. Both enantiomeric excess and diastereomeric ratio were determined by HPLC with an AD-H column at 220 nm (2-propanol:hexane=0.8:99.2), 1.0 mL/min; major enantiomer tmajor=43.3 min, minor enantiomer tminor=37.6 min. [α]D20=−21.1 (c=2.4, CHCl3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206090B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-ea5446a1628649f4a858ee2ab1659ecd |
| Source note | uspto-grants-2015_12 |