HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 25169813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | trans-4-Bromo-beta-nitrostyrene | HCID 688204 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 25169813 | HCID 25169813 | — |
Reaction Steps
The title compound was prepared from trans-1-bromo-4-(2-nitrovinyl)benzene and isobutyraldehyde according to general procedure. The enantiomeric excess was determined by HPLC with Chiralpak AD-H column at 210 nm (2-propanol:hexane=10:90), 1 mL/min; tmajor=11.5 min, tminor=9.3 min, [α]D20=−2.4 (c=2.9, CHCl3);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206090B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-41a9d03e68a34eb0a303d00891d0b892 |
| Source note | uspto-grants-2015_12 |