Triacetoxyperiodinane → HCID 86713198, compound

Participants

Reaction Steps

tert-Butyl (3-(5-bromopyridin-2-yl)-3-hydroxypropyl)carbamate(224 mg, 0.68 mmol) in ethylacetate (4.5 mL, 0.15 M) had 1.2 equivalents of Dess-Martin periodinane (344 mg, 0.81 mmol) added to it and stirred for 1 hour. The reaction mixture is then filtered and washed with sodium hydrogen carbonate and evaporated to give the title compound (220 mg): MS (ESI+) m/z 273.0 [M−But+H].

Provenance & Evidence