HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 117778323, compound → HCID 117778084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 117778323 | HCID 117778323 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 117778084 | HCID 117778084 | 95% |
Reaction Steps
Tert-butyl N-tert-butoxycarbonyl-N-{[3-(cyclopenten-1-yl)phenyl]methyl}carbamate (4.92 g) was dissolved in ethyl acetate (150 mL). To the solution, 10% palladium-carbon (0.50 g) was added, and the mixture was then stirred at room temperature for 2 hours under a hydrogen atmosphere. The reaction solution was filtered through celite. The filtrate was concentrated under reduced pressure to obtain the title compound (4.70 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206168B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-c7e065b040e74985b48cfac2733b5abb |
| Source note | uspto-grants-2015_12 |