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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1500500Generated: November 3, 2026

HCID 117778323, compound → HCID 117778084, compound

https://huagongshe.com/reaction/1500500

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 117778323HCID 117778323—
CatalystHCID 178418390HCID 178418390—
SolventEthyl AcetateHCID 8857—
ProductHCID 117778084HCID 11777808495%

Reaction Steps

Tert-butyl N-tert-butoxycarbonyl-N-{[3-(cyclopenten-1-yl)phenyl]methyl}carbamate (4.92 g) was dissolved in ethyl acetate (150 mL). To the solution, 10% palladium-carbon (0.50 g) was added, and the mixture was then stirred at room temperature for 2 hours under a hydrogen atmosphere. The reaction solution was filtered through celite. The filtrate was concentrated under reduced pressure to obtain the title compound (4.70 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09206168B2
Source datasetuspto-grants-2015_12
ORD IDord-c7e065b040e74985b48cfac2733b5abb
Source noteuspto-grants-2015_12