HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 71239220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 3096175 | HCID 3096175 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 71239220 | HCID 71239220 | — |
Reaction Steps
After sodium hydroxide (4.55 g) was dissolved in water (50 ml), 2,6-dichlorobenzylidenerhodanine (10.00 g) was added. The mixture was stirred under reflux for 5 hours, and then cooled to room temperature. The precipitated crystals were collected by filtration and washed with cold water to obtain sodium 4-chlorobenzo[b]thiophen-2-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206169B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-4294881bdb5747658b5817c28d1a57d2 |
| Source note | uspto-grants-2015_12 |