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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1500567Generated: October 31, 2026

HCID 11978936, compound → HCID 66886276, compound

https://huagongshe.com/reaction/1500567

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 11978936HCID 11978936—
ReactantEthanol hydrochlorideHCID 21887872—
SolventEthanolHCID 702—
ProductHCID 66886276HCID 66886276—

Reaction Steps

After 7-[3-(4-benzo[b]thiophen-4-yl-piperazin-1-yl)propoxy]-2-methyl-3,4-dihydro-2H-isoquinolin-1-one was made into an ethanol solution, 1N hydrochloric acid ethanol solution was added thereto, precipitated crystals were separated by filtration, recrystallized from ethanol and thereby 7-[3-(4-benzo[b]thiophen-4-yl-piperazin-1-yl)propoxy]-2-methyl-3,4-dihydro-2H-isoquinolin-1-one hydrochloride was obtained in the form of a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09206167B2
Source datasetuspto-grants-2015_12
ORD IDord-1da94268f25c4a428b68f28845018aed
Source noteuspto-grants-2015_12