HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-fluorobenzonitrile → HCID 89633331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-fluorobenzonitrile | HCID 2724900 | — |
| Reactant | HCID 89633494 | HCID 89633494 | — |
| Product | HCID 89633331 | HCID 89633331 | — |
Reaction Steps
(3R,9aS)-tert-butyl 3-(3-cyano-4-fluorophenyl)hexahydro-1H-pyrazino[1,2-a]pyrazine-2(6H)-carboxylate was synthesized following the procedure of (3R,9aS)-tert-butyl 3-((R)-3-methyl-1-oxoisochroman-6-yl)hexahydro-1H-pyrazino[1,2-a]pyrazine-2(6H)-carboxylate starting from 5-bromo-2-fluorobenzonitrile: LC/MS: (M+1)+: 361.17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09206199B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-fcbbd6b14f9e4c8884ee4f296e425e86 |
| Source note | uspto-grants-2015_12 |