HRID1502108

反应详情

EQUATION

反应方程式

HRID 1502108 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of ethyl (5-nitropyridin-2-yl)acetate (2.40 g, 11.4 mmol), Raney-Ni (50 mg) in 100 mL of MeOH was stirred at room temperature overnight. The mixture was filtered and concentrated to give ethyl (5-aminopyridin-2-yl)acetate.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. concentrationconcentrated