Water → HCID 66717381, compound

Participants

Reaction Steps

The obtained 3,6-diphenyl-9-(4-hydroxyphenyl)carbazole (1.54 g, 3.7 mmol) was dissolved in N,N-dimethylformamide (20 mL). Under cooling with ice water, 55% by mass sodium hydride (0.25 g, 5.7 mmol) was added to the resultant solution, followed by stirring for 1 hour. Next, 8-bromo-1-octanol (1.16 g, 5.5 mmol) was added thereto, and the resultant mixture was stirred for 3 hours at room temperature. In addition, the mixture was poured to water, followed by extraction with ethyl acetate. Next, the mixture was washed with water and dried and the solvent was evaporated, to thereby obtain 1.90 g of 8-[4-(3,6-diphenylcarbazol-9-yl)phenoxy]octan-1-ol.

Provenance & Evidence